Preparation of New Hybrid Materials SiO2@Melamine-Cyanurate as Precursors of Graphite-Like Carbon Nitride

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Abstract

This work describes the use of silica particles obtained by sol-gel method as a templat for deposition of supramolecular complexes of melamine cyanurate. To obtain SiO2@melamine-cyanurate (SiO2@MCA) material, the method of covalent modification of silica surface by melamine molecules (SiO2-mel) was applied and the method of its further functionalization by hydrogen-bonded organic framework of melamine-cyanurate (HOF, MCA) was proposed. One of the promising directions of using SiO2@melamine-cyanurate is obtaining SiO2@g-C3N4 material on its basis. Control of the amount of applied melamine-cyanurate allows to potentially obtain g-C3N4 layers of different thicknesses on the silica surface.

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About the authors

М. D. Lebedev

Ivanovo State University of Chemistry and Technology

Author for correspondence.
Email: MaximLebedev37@gmail.com
Russian Federation, Ivanovo, 153000

A. A. Goncharenko

Ivanovo State University of Chemistry and Technology

Email: MaximLebedev37@gmail.com
Russian Federation, Ivanovo, 153000

I. A. Skvortsov

Ivanovo State University of Chemistry and Technology

Email: ivanskvortsov@mail.ru
Russian Federation, Ivanovo, 153000

M. S. Kuzmikov

Ivanovo State University of Chemistry and Technology; Krestov Institute of Solution Chemistry of the Russian Academy of Sciences

Email: MaximLebedev37@gmail.com
Russian Federation, Ivanovo, 153000; Ivanovo, 153045

A. S. Vashurin

Ivanovo State University of Chemistry and Technology

Email: MaximLebedev37@gmail.com
Russian Federation, Ivanovo, 153000

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Supplementary files

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2. Fig. 1. SEM images of materials: a – SiO2-MCA 25%; b – SiO2-MCA 50%.

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3. Fig. 2. Thermograms of MCA, SiO2-MCA 50% and SiO2-MCA 25%.

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4. 3. X-ray diffractograms of MCA, SiO2-MCA 50% and SiO2-MCA 25%.

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5. Fig. 4. IR spectra of MCA, SiO2-mel, SiO2-MCA 25% and SiO2-MCA 50%.

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6. Fig. 5. Raman spectra of MCA, SiO2-mel, SiO2-MCA 25% and SiO2-MCA 50%.

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