Synthesis, structure and optical properties of semiconductor perovskite nanoparticles CsBX3 (B = Pb, Mn; X = Br, Cl)

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Currently, ABX3 nanoparticles (NPs) based on lead halides attract the attention due to their unique optical properties and a wide range of applications. The preparation of NPs with lead as a partial or complete replacement is particularly interesting because of the toxicity of this chemical element and most of its compounds. In this study, we propose a modified method for perovskite NPs synthesis using manganese as a partial replacement for lead. The results obtained describe the structures, shapes and dimensions of the synthesized nanoparticles. It has been shown that partial replacement of lead with manganese leads to the appearance of new photoluminescence bands in the region of 600 nm.

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作者简介

V. Gushchina

Moscow Institute of Physics and Technology (National Research University); Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: ya.l2er0us0ya2012@ya.ru
俄罗斯联邦, Dolgoprudny, 141701; Moscow, 119991

A. Son

Moscow Institute of Physics and Technology (National Research University); Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

编辑信件的主要联系方式.
Email: sonsacha@gmail.com
俄罗斯联邦, Dolgoprudny, 141701; Moscow, 119991

A. Egorova

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
俄罗斯联邦, Moscow, 119991

A. Arkhipenko

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
俄罗斯联邦, Moscow, 119991

M. Teplonogova

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
俄罗斯联邦, Moscow, 119991

N. Efimov

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
俄罗斯联邦, Moscow, 119991

S. Kozyukhin

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

Email: sonsacha@gmail.com
俄罗斯联邦, Moscow, 119991

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2. Рис.1. ② : 1 – cspbbr3; 2 – cspbcl3–zbrz; 3 – cspbcl3; 4 – cspb1–ymnycl3–Zbrz; 5 – Cspb1–ymnycl3.

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3. Рис. 2. Микрофотографии наночастиц различных составов: CsPbBr3 (а); CsPbCl3–zbr you (б); CsPbCl3 (в); CsPb1–yMnyCl3–zbr you (г); CsPb1–yMnyCl3 (д).

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4. Fig. 3. ② : 1 – cspbbr3; 2 – cspbcl3–zbrz; 3 – cspbcl3; 4 – cspb1–ymnycl3–zbrz; 5 – Cspb1–Ymnycl3.

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5. Fig. 4. 6-cspbbr3; 2 – cspbcl3 – zbrz; 3–cspbcl3; 4 – cspb1 – ymnycl3–zbrz; 5–cspb1 – ymnycl3.

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6. Fig. 5. Photoluminescence spectra of nanoparticles: 1 – CsPbBr3 (λvozb = 365 nm); 2 – CsPbCl3–zBrz (λvozb = = 365 nm); 3 – CsPbCl3 (λvozb = 365 nm); 4 – CsPb1–yMnyCl3–zBrz (λvozb = 227 nm); 5 – CsPb1–yMnyCl3 (λvb = 241 nm).

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7. Fig. 6. EPR spectra for CsPb1–yMnyCl3 nanoparticles (X-band, 294 K).

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